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Development of an In-situ Environmental Fluid Cell for Synchrotron X-ray…

Award Information

Agency:
Department of Energy
Branch:
N/A
Award ID:
Program Year/Program:
2013 / SBIR
Agency Tracking Number:
83495
Solicitation Year:
2013
Solicitation Topic Code:
03 d
Solicitation Number:
DE-FOA-0000760
Small Business Information
Hummingbird Precision Machine Co, Dba Hummingbird
8300 28th Ct. St. Unit 200 Lacey, WA 98516-7126
View profile »
Woman-Owned: No
Minority-Owned: No
HUBZone-Owned: No
 
Phase 1
Fiscal Year: 2013
Title: Development of an In-situ Environmental Fluid Cell for Synchrotron X-ray Microscopy
Agency: DOE
Contract: DE-FG02-13ER90601
Award Amount: $150,000.00
 

Abstract:

Observing solid-liquid interfaces with high resolution is important for comprehension of physical, chemical and biological interactions between material and fluid. A more detailed knowledge of these interactions can substantially improve our understanding of the processes that occur during operation of catalysts and degradation of materials inside battery, as well as the operation of biological systems. Currently, a few liquid stages at synchrotrons have been home- built and suffer from leaks, are extremely cumbersome to use and do not provide any additional capabilities such as electrical biasing and heating of the sample. Failures of these liquid cells make experiments extremely challenging to carry out and in some cases endanger surrounding equipment. Our approach will be to develop a continuous flow environmental cell specifically for X-ray microscopes that will allow operation of the sample in liquid and gas at a wide range of pressures. Dynamic in-situ experiments are finding increasing use as direct methods to explore the relationships among materials processing methods, microstructure and functional properties. X-ray microscopy can provide information about changes in chemical structure of materials with high spatial resolution during dynamic in-situ experiments. Many processes such as degradation of materials, charging/discharging of batteries, operation of cells/bacteria can be studied with X-ray microscopy and are of a great importance to academic as well as industrial research. The proposed platform provides a tool to study such changes in the chemical structure of materials.

Principal Investigator:

Norman Salmon
Mr.
3602522737
norman@hummingbirdscientific.com

Business Contact:

Norman Salmon
Mr.
norman@hummingbirdscientific.com
Small Business Information at Submission:

Hummingbird Precision Machine Co, Dba Hummingbird
8300 28th Ct NE Unit 200 Lacey, WA 98516-7126

EIN/Tax ID: 262122444
DUNS: N/A
Number of Employees:
Woman-Owned: No
Minority-Owned: No
HUBZone-Owned: No