An Elevated-Temperature Nanobalance Based on Piezoelectric Shear Mode Resonators (quartz, gallium phosphate, and langasite)

Award Information
Agency: Department of Commerce
Branch: National Institute of Standards and Technology
Contract: SB1341-08-SE-0670
Agency Tracking Number: 504-08
Amount: $90,000.00
Phase: Phase I
Program: SBIR
Solicitation Topic Code: N/A
Solicitation Number: N/A
Timeline
Solicitation Year: N/A
Award Year: 2008
Award Start Date (Proposal Award Date): N/A
Award End Date (Contract End Date): N/A
Small Business Information
PO Box 137491, Clermont, FL, 34713
DUNS: N/A
HUBZone Owned: N
Woman Owned: N
Socially and Economically Disadvantaged: N
Principal Investigator
 Allan Smith
 (863) 588-1693
 allan.smith@masscal.com
Business Contact
Phone: () -
Research Institution
N/A
Abstract
The work proposed will provide a demonstration of feasibility and specific design recommendations for building an elevated-temperature resonating crystal balance with nanogram sensitivity. The approach will build upon existing technology commercialized by Masscal for operating a QCM in a temperature-controlled calorimeter. Precise temperature control and new types of crystal sensors will be used to greatly extend the temperature range of operation, reduce measurement errors at higher temperatures, and increase practical usability of the final product. In Phase I, we will (1) demonstrate current capability in gases under 100°C; (2) extend the capability to include aqueous solutions up to 85°C (3) fabricate new candidate crystal sensors from quartz, gallium phosphate and langasite for operation up to 250°C and then further to 600°C; (4) design and assemble a breadboard instrument and use it to perform preliminary testing of new sensors; (5) develop specific recommendations for a high-temperature instrument up to 600°C; and (6) demonstrate capabilities by measuring oxidation in a nanostructured thin film from NIST up to 250°C.

* Information listed above is at the time of submission. *

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