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High Temperature Material Coatings

Award Information
Agency: Department of Defense
Branch: Navy
Contract: N68335-14-C-0121
Agency Tracking Number: N132-146-0486
Amount: $80,000.00
Phase: Phase I
Program: SBIR
Solicitation Topic Code: N132-146
Solicitation Number: 2013.2
Solicitation Year: 2013
Award Year: 2014
Award Start Date (Proposal Award Date): 2014-02-11
Award End Date (Contract End Date): 2014-08-11
Small Business Information
4401 Dayton-Xenia Road
Dayton, OH 45432-1894
United States
DUNS: 074689217
HUBZone Owned: No
Woman Owned: Yes
Socially and Economically Disadvantaged: No
Principal Investigator
 Emmanual Boakye
 Principal Investigator
 (937) 426-6900
Business Contact
 Rick Weddle
Title: Director, Contracts
Phone: (937) 426-6900
Research Institution

Hf-based thick refractory coatings will be developed on existing carbon substrates including C-C composites to improve its oxidation resistance at 3200-5000F. A wet-chemical synthesis approach to preparing HfB2VC mixtures will be used which lends itself ideally to control the HfB2VC mixtures and afford a graded coating with carbon rich inner-coat, and HfB2 rich outer coat. A HfO2 outer layer will be deposited on the composite. A dense tetragonal-stabilized HfO2 over coat will provide more protection.. Elements of stabilization include tungsten (W), molybdenum (Mo), and yttrium (Y). Further, W and Mo will also serve as an in-situ sintering aid for HfO2. The HfB2 phase will provide supplementary protection if any failure should occur in the original HfO2 outer layer. Samples will be tested by the use of an oxyacetylene torch test to evaluate temperatures to 5000aF. Successful tests will include samples that are able to withstand multiple thermal cycles without cracking and have low erosion depths.

* Information listed above is at the time of submission. *

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