Automated Polychlorinated Biphenyl (PCB) Analyzer for Solid Waste Material using SPME/GC/MS

Award Information
Agency:
Department of Defense
Branch
Navy
Amount:
$70,000.00
Award Year:
2004
Program:
SBIR
Phase:
Phase I
Contract:
N65538-04-M-0131
Award Id:
70112
Agency Tracking Number:
N041-100-1107
Solicitation Year:
n/a
Solicitation Topic Code:
n/a
Solicitation Number:
n/a
Small Business Information
1981Pine Hall Drive, State College, PA, 16801
Hubzone Owned:
N
Minority Owned:
N
Woman Owned:
N
Duns:
118955538
Principal Investigator:
Venkat Mani
R&D Director
(814) 234-7074
vmani101@yahoo.com
Business Contact:
Venkat Mani
R&D Director
(814) 234-0123
vmani@americananalytical.us
Research Institute:
n/a
Abstract
The main goal of this Phase I SBIR proposal is to demonstrate the feasibility of developing an automated method that can be used in the field to identify and quantify polychlorinated biphenyl compounds (PCBs) present in solid materials felt gasket, faying material, paint, electric power cable insulation and many rubber products. Solid Phase Microextraction (SPME) has been shown to be effective in the determination of the concentration of PCBs in liquids. In this modified SPME technique, new stable fibers with nano particles will be developed for efficient and selective absorption of PCBs. Modified fiber holders will be developed to automate the accurate determination of the presence and concentration of PCB's in solid materials. This will be a quick, reliable, cost effective and portable device that can be operated in the field by a single person with minimum training. The sensitivity reached with this technique is 5-700 parts per trillion ( EPA regulation 50 parts per million) in an extraction time of only 50 minutes. The sensitivity, extraction parameters and time for analysis will be improved in this proposal. This proposal will also enable the separation and quantitation of toxic PCB congeners and highly toxic polychlorodibenzofurans (PCDF) and dioxins produced from PCBs. This proposal combines SPME with portable GC and/or GC/MS for automated PCB analysis.

* information listed above is at the time of submission.

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